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- W1548100377 abstract "The research conducted can be split into three major regions; pigmentmaterial, a simulation program called QuadFit and mesoporous oxides. Therehas also been some extra work conducted on a catalyst for partial hydrogenationof vegetable oils. Various techniques have been used on the different systemsincluding XPS, STEM and 77Se, 17O, 93Nb, 15N, 119Sn, 27Al, 115In and 63,65Custatic and MAS NMR.The pigment materials consist of a series of materials which are groupedunder the F-Colours project. The pigments consist of sulphur doped tin niobates,copper indium sulphur selenide doped zinc selenides, sulphur doped tin tungstatesand colloidal gold and silver enamels. The sulphur doped tin niobate study showsa conversion from foordite to pyrochlore and also where the sulphur sits in thestructure. The copper indium sulphur selenide doped zinc selenide study shows theindium and copper moving into the zinc selenide as copper indium pairs. However,how the pairs sit in the structure remains undetermined. The sulphur doped tintungstate study shows that the sulphur acts as a promoter for the beta phaserather than the desired alpha phase. The enamels based on gold and silver showthat the tin site does not determine the colour of the enamel and the silver-goldassociation is likely to be the dominant factor.Mesoporous oxides show a link between the amount of mesoporous structureand their temperature stability. The nitrogen spectra of the template in thematerial shows that in the mesoporous silicate (which has the largest surface area)there is a breakdown of the amine into NH groups which does not appear in theother mesoporous materials. This could lead to a method of increasing the surfacearea of the other mesoporous oxides.QuadFit has the ability to simulate quadrupolar and CSA interactions withdistributions of interactions whilst static and the quadrupolar interaction withdistributions under MAS. The program is written in Java so will run on mostplatforms and also has near perfect stability." @default.
- W1548100377 created "2016-06-24" @default.
- W1548100377 creator A5065112315 @default.
- W1548100377 date "2008-01-01" @default.
- W1548100377 modified "2023-09-27" @default.
- W1548100377 title "Solid state NMR studies of inorganic pigment materials and catalysts" @default.
- W1548100377 hasPublicationYear "2008" @default.
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