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- W1551754483 abstract "Pb/sup 210/ in equilibrium with lead carrier, was co-prectpitated from effluent with strontium sulfate. The precipptate was metathesised to the carbonate, dissolved in dilute hydrochloric acid and the lead chloro-complex was absorbed on a column of anion exchange resin. The lead was eluted, precipitated as the chromate and beta -counted after allowing time for the Bi/sup 210/ daughter to grow in (5-day half-life). The activity of the precipitate, after corrections for chemical yield and ingrowth were made, was compared with the activity of similar sources prepared from a standardized solution of Pb/sup 210/. Decontamination factors at this stage were high, but improved separation from interfertng nuclides could be achieved by dissolving the lead chromate in the presence of bismuth carrmer and repeating the anion exchange separation. The lead fraction was rejected. The bismuth was recovered, precipitated as the phosphate, and beta -counted. (auth)" @default.
- W1551754483 created "2016-06-24" @default.
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- W1551754483 date "1961-08-01" @default.
- W1551754483 modified "2023-09-27" @default.
- W1551754483 title "THE DETERMINATION OF LEAD-210 IN HARWELL EFFLUENT" @default.
- W1551754483 hasPublicationYear "1961" @default.
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