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- W1553863189 abstract "Abstract A reliable and generally applicable synthetic route for the rational synthesis of silicon‐centered tripod ligands with mixed dialkylphosphine/diarylphosphine donors is developed. On the basis of this protocol, two new asymmetric SiPPP′ ligands, SiP Me 2 P Ph and SiP Me 2 P i Pr , were prepared and employed for the synthesis of (dinitrogen)molybdenum complexes of the types [Mo(N 2 )(SiPPP′)(P 2 )] [P 2 = (diphenylphosphino)methane (dppm), (dimethylphosphino)methane (dmpm), or two PMe 2 Ph] and [Mo(N 2 ) 2 (SiPPP′)(PMe 2 Ph)]. The constitution of the complexes is elucidated by 31 P NMR spectroscopy and analyzed on the basis of steric and electronic factors. The activation of N 2 in the synthesized dinitrogen complexes is determined by IR spectroscopy and correlated with the donor/acceptor properties of the phosphine coligands." @default.
- W1553863189 created "2016-06-24" @default.
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- W1553863189 date "2014-07-04" @default.
- W1553863189 modified "2023-10-10" @default.
- W1553863189 title "(Dinitrogen)molybdenum Complexes Supported by Asymmetric Silicon‐Centered Tripod Ligands: Steric and Electronic Influences on the Coordination of Mono‐ and Diphosphine Coligands" @default.
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- W1553863189 doi "https://doi.org/10.1002/ejic.201402273" @default.
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