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- W1554443706 abstract "Reversed-phased thin-layer chromatography of sterioids. I. Measurement and interpretation of RM values. RM values of about one hundred steroids with hetero substituents have been measured, using reversed-phase thin-layer chromatography. Silica gel (PF254)-silanised served as the stationary non-polar phase and acetone in various mixtures with water as the mobile polar phase. The ΔRM values of substituents have been calculated and correlated with different parameters of hydrophobicity (πar, πal,VI). Neighbouring effects were investigated. Die RM-Werte von ungefähr 100 Steroidhormonanaloga wurden mittels “reversed-phase”-Dünnschichtchromatographie bestimmt. Als stationäre unpolare Phase wurde silanisiertes Kieselgel (PF254-silanisiert) und als mobile polare Phase Aceton in verschiedenen Mischungsverhältnissen mit Wasser verwendet. Von einer Reihe von Substituenten wurde die ΔRM-Werte in Abhängigkeit von Nachbargruppen berechnet. Die ΔRM-Werte korrelieren signifikant mit anderen Hydrophobizitätsparametern (πar, πal,Vl). Dabie ergeben die ΔRM-Werte bezüglich 45% Aceton im Gegensatz zu denen bezüglich 0% Aceton bessere Resultate. Aus den Regressionsgleichungen konnten Aussagen zu der aus Wasser und Aceton bestehenden Mischsolvathülle abgeleitet und weitere Polaritätsinkremente (VH) berechmnet werden" @default.
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- W1554443706 date "1981-01-01" @default.
- W1554443706 modified "2023-09-29" @default.
- W1554443706 title "“Reversed-phase”-dünnschichtchromatographie von steroiden" @default.
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- W1554443706 doi "https://doi.org/10.1016/s0021-9673(00)81819-1" @default.
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