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• W1556446088 abstract "Prolonged photolysis of aqueous solution containing [V4O12]4− and MeOH at pH 5.5 in the presence of K2MoO4 leads to the formation of K6H2[V22O54(MoO4)]⋅19H2O (1). The anion of 1, formally written as [VIV8VV14O54(MoO4)]8−, forms cluster shell with approximate D2d symmetry as a subgroup of Td symmetry for MoO42−. The interaction of the oblong and egg-shaped {V22O54} cluster shell encapsulated by MoO42− is stronger than that of the ClO4−-encapsulated anion with the same topology but there is still no significant bonding of the shell V atoms to the template O atoms (with V⋅⋅⋅O(Mo) distances of >2.7 Å). The template-exchange reaction of [VIV18O42(H2O)]12− with small anions occurs via oxidative splitting of VIV–O–VIV bond of the shell cluster to yield the mixed-valent polyoxovanadate clusters, the structure of which reflects symmetry, charge, and disorder of the central anion template." @default.
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• W1556446088 date "1999-11-01" @default.
• W1556446088 modified "2023-10-16" @default.
• W1556446088 title "Photochemical self-assembly reactions of polyoxovanadates" @default.
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• W1556446088 doi "https://doi.org/10.1016/s1381-1169(99)00142-9" @default.
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