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- W1562304823 abstract "Abstract The sign of the side-chain spin coupling JCHO-3 in 2-hydroxy-5-methoxy-benzaldehyde has been determined relative to that of the ring coupling constants by use of a nuclear magnetic double resonance technique. Strong non-selective double irradiation was applied in the ABC-part (the ring hydrogen band) of the spectrum to produce a sign dependent asymmetry in the X-part (the aldehyde band) of the spectrum. The results were interpreted with the aid of theoretical double resonance spectra calculated by complete numerical diagonalization of the double resonance Hamiltonian matrix. It was found that JCHO-3 carries the same sign as the ring coupling constants." @default.
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- W1562304823 date "1965-07-01" @default.
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- W1562304823 title "Nuclear magnetic double resonance in an ABCX spin system" @default.
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- W1562304823 doi "https://doi.org/10.1016/0022-2852(65)90106-2" @default.
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