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- W1563001572 abstract "Since 1995 several groups have shown that indeed the synthesis of nanoporous transition metal oxides via supramolecular liquid crystalline templating is possible for TiCh [1,2], Z1O2 [2-4], Nb2O5 [2,5], Ta2O5 [6] and Mn3O4 [7]. Here we present some strategies to enhance the quality of existing materials and to expand the variety in composition. The synthesis and characterization of mesostructured titanium, rhenium and chromium oxides are presented. In case of titania the often used precursor Ti(O'Pr)4 has been modified with different chelating agents such as dioles, etheralcohols and β-diketones. At high surfactant concentration the addition of these modifiers revealed to be unnecessary. In order to obtain unprecedented mesostructured rheniumdioxide, methyltrioxorhenium (MTO), a special organometallic precursor was used. For the synthesis of mesostructured chromium (III) oxide a cluster compound containing three chromium ions showed up to be of the greatest benefit. For all systems several types of surfactants were tested. Products were characterised by P-XRD, TEM, REM, EDX, XAFS, TG/DTA and physisorption measurements." @default.
- W1563001572 created "2016-06-24" @default.
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- W1563001572 date "2000-01-01" @default.
- W1563001572 modified "2023-09-26" @default.
- W1563001572 title "On the Way to New Nanoporous Transition Metal Oxides" @default.
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- W1563001572 doi "https://doi.org/10.1016/s0167-2991(00)80234-7" @default.
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