FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W1566547551> ?p ?o ?g. }

• W1566547551 endingPage "321" @default.
• W1566547551 startingPage "317" @default.
• W1566547551 abstract "A new technique for sample preparation on-line with LC and GC–MS assays was developed. Microextraction in a packed syringe (MEPS) is a new miniaturised, solid-phase extraction technique that can be connected on-line to GC or LC without any modifications. In MEPS approximately 1 mg of the solid packing material is inserted into a syringe (100–250 μl) as a plug. Sample preparation takes place on the packed bed. The bed can be coated to provide selective and suitable sampling conditions. The new method is very promising. It is very easy to use, fully automated, of low cost and rapid in comparison with previously used methods. This paper presents the development and validation of a method for microextraction in packed syringe MEPS on-line with GC–MS. Local anaesthetics in plasma samples were used as model substances. The method was validated and the standard curves were evaluated by the means of quadratic regression and weighted by inverse of the concentration: 1/x for the calibration range 5–2000 nM. The applied polymer could be used more than 100 times before the syringe was discarded. The extraction recovery was between 60 and 90%. The results showed close correlation coefficients (R>0.99) for all analytes in the calibration range studied. The accuracy of MEPS–GC–MS was between 99 and 115% and the inter-day precision (n=3 days), expressed as the relative standard deviation (R.S.D.%), was 3–10%." @default.
• W1566547551 created "2016-06-24" @default.
• W1566547551 creator A5037654890 @default.
• W1566547551 date "2004-03-01" @default.
• W1566547551 modified "2023-10-17" @default.
• W1566547551 title "New trend in sample preparation: on-line microextraction in packed syringe for liquid and gas chromatography applications" @default.
• W1566547551 cites W1515542254 @default.
• W1566547551 cites W1968337414 @default.
• W1566547551 cites W1990852254 @default.
• W1566547551 cites W1999414834 @default.
• W1566547551 cites W2000166050 @default.
• W1566547551 cites W2017920890 @default.
• W1566547551 cites W2018446129 @default.
• W1566547551 cites W2029834002 @default.
• W1566547551 cites W2035111838 @default.
• W1566547551 cites W2046196649 @default.
• W1566547551 cites W2066657617 @default.
• W1566547551 cites W2068966336 @default.
• W1566547551 cites W2086663941 @default.
• W1566547551 cites W2332454355 @default.
• W1566547551 doi "https://doi.org/10.1016/j.jchromb.2003.11.042" @default.
• W1566547551 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/14751801" @default.
• W1566547551 hasPublicationYear "2004" @default.
• W1566547551 type Work @default.
• W1566547551 sameAs 1566547551 @default.
• W1566547551 citedByCount "351" @default.
• W1566547551 countsByYear W15665475512012 @default.
• W1566547551 countsByYear W15665475512013 @default.
• W1566547551 countsByYear W15665475512014 @default.
• W1566547551 countsByYear W15665475512015 @default.
• W1566547551 countsByYear W15665475512016 @default.
• W1566547551 countsByYear W15665475512017 @default.
• W1566547551 countsByYear W15665475512018 @default.
• W1566547551 countsByYear W15665475512019 @default.
• W1566547551 countsByYear W15665475512020 @default.
• W1566547551 countsByYear W15665475512021 @default.
• W1566547551 countsByYear W15665475512022 @default.
• W1566547551 countsByYear W15665475512023 @default.
• W1566547551 crossrefType "journal-article" @default.
• W1566547551 hasAuthorship W1566547551A5037654890 @default.
• W1566547551 hasConcept C10390740 @default.
• W1566547551 hasConcept C105795698 @default.
• W1566547551 hasConcept C113196181 @default.
• W1566547551 hasConcept C118552586 @default.
• W1566547551 hasConcept C119128265 @default.
• W1566547551 hasConcept C123460561 @default.
• W1566547551 hasConcept C15744967 @default.
• W1566547551 hasConcept C162356407 @default.
• W1566547551 hasConcept C165838908 @default.
• W1566547551 hasConcept C185592680 @default.
• W1566547551 hasConcept C205345274 @default.
• W1566547551 hasConcept C23531484 @default.
• W1566547551 hasConcept C2778533135 @default.
• W1566547551 hasConcept C2778571141 @default.
• W1566547551 hasConcept C2778576202 @default.
• W1566547551 hasConcept C33923547 @default.
• W1566547551 hasConcept C43617362 @default.
• W1566547551 hasConcept C4725764 @default.
• W1566547551 hasConcept C50712719 @default.
• W1566547551 hasConcept C81426234 @default.
• W1566547551 hasConceptScore W1566547551C10390740 @default.
• W1566547551 hasConceptScore W1566547551C105795698 @default.
• W1566547551 hasConceptScore W1566547551C113196181 @default.
• W1566547551 hasConceptScore W1566547551C118552586 @default.
• W1566547551 hasConceptScore W1566547551C119128265 @default.
• W1566547551 hasConceptScore W1566547551C123460561 @default.
• W1566547551 hasConceptScore W1566547551C15744967 @default.
• W1566547551 hasConceptScore W1566547551C162356407 @default.
• W1566547551 hasConceptScore W1566547551C165838908 @default.
• W1566547551 hasConceptScore W1566547551C185592680 @default.
• W1566547551 hasConceptScore W1566547551C205345274 @default.
• W1566547551 hasConceptScore W1566547551C23531484 @default.
• W1566547551 hasConceptScore W1566547551C2778533135 @default.
• W1566547551 hasConceptScore W1566547551C2778571141 @default.
• W1566547551 hasConceptScore W1566547551C2778576202 @default.
• W1566547551 hasConceptScore W1566547551C33923547 @default.
• W1566547551 hasConceptScore W1566547551C43617362 @default.
• W1566547551 hasConceptScore W1566547551C4725764 @default.
• W1566547551 hasConceptScore W1566547551C50712719 @default.
• W1566547551 hasConceptScore W1566547551C81426234 @default.
• W1566547551 hasIssue "2" @default.
• W1566547551 hasLocation W15665475511 @default.
• W1566547551 hasLocation W15665475512 @default.
• W1566547551 hasOpenAccess W1566547551 @default.
• W1566547551 hasPrimaryLocation W15665475511 @default.
• W1566547551 hasRelatedWork W2000935814 @default.
• W1566547551 hasRelatedWork W2005102210 @default.
• W1566547551 hasRelatedWork W2032719152 @default.
• W1566547551 hasRelatedWork W2034733834 @default.
• W1566547551 hasRelatedWork W2165368246 @default.
• W1566547551 hasRelatedWork W2761385196 @default.
• W1566547551 hasRelatedWork W4241145609 @default.
• W1566547551 hasRelatedWork W4292466628 @default.
• W1566547551 hasRelatedWork W4296717893 @default.
• W1566547551 hasRelatedWork W44437537 @default.
• W1566547551 hasVolume "801" @default.
• W1566547551 isParatext "false" @default.
• W1566547551 isRetracted "false" @default.

• next