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- W1567018644 abstract "Twelve new chiral cyclopentadienyl-titanium or -zirconium complexes Cp′2TiCl2, Cp′CpTiCl2 and Cp′2ZrCl2, (Cp = η5-cyclopentadienyl and Cp′ = CH3OCH(R′) CH(R′')Cp), have been synthesized. Complex (R,R)-1 have been studied by X-ray analysis. The complex (R,R)-1 forms violet-red plate crystals, which are triclinic, space group P1, with a 6.775(3), b 6.792(4), c 35.517(22) A, α 89.94(5), β90.05(4), γ 119.98(4)°, V 1415(1) A3, Z = 3. The structure was refined to an R factor of 0.039 for 3142 observed reflections. The complex (R,R-3 forms colorless plate crystals, and is isomorphous with (R,R)-1, a 6.8295(6), b 6.8301(6), c 35.940(2) A, α 89.990(7), β 90.011(7), γ 119.997(6)°, V 1541.9(2) A3. The final R factor is 0.065 for 2608 observed reflections." @default.
- W1567018644 created "2016-06-24" @default.
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- W1567018644 date "1989-06-01" @default.
- W1567018644 modified "2023-09-28" @default.
- W1567018644 title "Organotitanium chemistry" @default.
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- W1567018644 doi "https://doi.org/10.1016/0022-328x(89)85405-1" @default.
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