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• W1568082126 endingPage "1932" @default.
• W1568082126 startingPage "1926" @default.
• W1568082126 abstract "The application of 13-C nuclear magnetic resonance to the analysis of some sialic acid-containing meningococcal polysaccharide antigens is described. Complete assignments of the spectra of both the native serogroup B and the de-O-acetylated serogroup C polysaccharides have been made. These assignments were based on the corresponding data for some related monomers (sialic acid and its alpha-and beta-methylglycosides) and on supportive chemical evidence. The data indicate that the serogroup B polysaccharide is a 2 yields 8-alpha-linked homopolymer of sialic acid, identical in structure with colominic acid from Escherichia coli, whereas the de-O-acetylated serogroup C polysaccharide is a 2 yield 9-alpha-linked homopolymer. The native serogroup C polysaccharide is O-acetylated (1.16 mol of O-acetyl per sialic acid residue), all the O-acetyl substituents being located only at C-7 and C-8 of the sialic acid residues, and in addition contains unacetylated residues (24%). The polysaccharide contains di-O-acetylated residues (O-acetyl on C-7 and C-8), and at least one of the possible monoacetylated residues at C-7 or C-8." @default.
• W1568082126 created "2016-06-24" @default.
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• W1568082126 date "1975-03-01" @default.
• W1568082126 modified "2023-10-10" @default.
• W1568082126 title "Structural determination of the sialic acid polysaccharide antigens of Neisseria meningitidis serogroups B and C with carbon 13 nuclear magnetic resonance." @default.
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• W1568082126 doi "https://doi.org/10.1016/s0021-9258(19)41784-5" @default.
• W1568082126 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/163259" @default.
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