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- W1568575054 abstract "Die Struktur der Titelsubstanz 2 d wurde röntgenographisch aus Diffraktometer-Einkristalldaten bestimmt und bis zu einem konventionellen R von 0,038 verfeinert. Der 8-Ring besitzt Sessel-Sessel-Konformation mit transannularer 1,5-Sb …︁ O-Annäherung. Die Koordination am Sb-Atom ist ψ-trigonal-bipyramidal mit äquatorialen Abständen SbS 244 pm und axialen Abständen SbCl 245 und SbO 253 pm. Relative Bindungsordnungen der transannularen Akzeptor-Donator-Wechselwirkung in 2 d und analogen Heterocyclen werden diskutiert. Die 2 d-Molekeln sind 12fach koordiniert. On Heterocyclic Systems Containing Antimony. II [1]. Molecular and Crystal Structure of 5-Chloro-1-oxa-4,6-dithia-5-stibocane The crystal structure of the title compound 2 d has been determined from single crystal X-ray data and refined to a conventional R of 0.038. The eight-membered ring has the chair-chair conformation with 1,5-transannular Sb …︁ O-interaction. The coordination of the Sb-atom is ψ-trigonal-bipyramidal with equatorial distances SbS 244 pm and axial distances SbCl 245 and SbO 253 pm. Correlated bond orders for the transannular acceptor-donor interaction in 2 d and analogous heterocycles are discussed. The 2 d-molecules are 12-coordinated." @default.
- W1568575054 created "2016-06-24" @default.
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- W1568575054 date "1976-07-01" @default.
- W1568575054 modified "2023-10-16" @default.
- W1568575054 title "�ber Antimon-haltige Heterocyclen. II [1]. Molek�l- und KristallStruktur von 5-Chlor-1-oxa-4,6-dithia-5-stibocan" @default.
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- W1568575054 doi "https://doi.org/10.1002/zaac.19764240213" @default.
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