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- W1569070162 abstract "Analysis of product formation reveals that in the reaction of iodomethane and magnesium in anyl phenyl ether ethane and 1-butane are the major side products. The latter product is formed mainly by addition of methyl radicals to the terminal CH2 group of allyl phenyl ehter, followed by β-scission under extrusion of a phenoxy radical. This mechanismf is confirmed by an analysis of the CIDNP spectra during the reaction; CH3 radicals escaping from CH3 CH3 pairs and adding to allyl phenyl ether give rise to a very clear example of a second order CIDNP spectrum in the product 1-butane, while polarization in CH3C6H5O-CH-CHCH2 pairs, formed after α-H abstraction from allyl phenyl ether, leads to net effects in the products ethane (E) and 1-methylallyl phenyl ether (A)." @default.
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- W1569070162 date "1978-01-01" @default.
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- W1569070162 title "The formation of grignard compounds—V" @default.
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- W1569070162 doi "https://doi.org/10.1016/0040-4020(78)88381-1" @default.
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