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• W1569088598 abstract "Novel η1-vinyl complexes of the type Cp(CO)(L)FeC(OMe)C(R)R′ (R = R′ = H, Me; R = H, R′ = Me; L = Me3P, Ph3P) are obtainied via methylation of the acyl complexes Cp(CO)(L)FeC(O)R (R = Me, Et, i-Pr) with MeOSO2F and subsequent deprotonation of the resulting carbene complexes [Cp(CO)(L)FeC(OMe)R]SO3F with the phosphorus ylide Me3PCH2. The same procedure can be applied for the synthesis of the pentamethylcyclopentadienyl derivative C5Me5(CO)(Me3P)FeC(OMe)CH2, while treatment of the hydroxy or siloxy carbene complexes [Cp(CO)(L)FeC(OR)Me]X (R = H, Me3Si; X = SO3CF3) with Me3CH2 results in the transfer of the oxygen bound electrophile to the ylidic carbon. Some remarkable spectroscopic properties of the new complexes are reported." @default.
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• W1569088598 date "1983-04-01" @default.
• W1569088598 modified "2023-10-18" @default.
• W1569088598 title "Zur reaktion von metall-koordiniertem kohlenmonoxid mit yliden" @default.
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• W1569088598 doi "https://doi.org/10.1016/0022-328x(83)80206-x" @default.
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