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- W1569093682 abstract "Treatment of 2-methyl-6,7-methylenedioxy-3,4-dihydroisoquinolinium perchlorate (7) with diazomethane afforded a mixture of aziridinium salts (8 + 9) which underwent reaction with MeOH to produce the 1,2,4,5-tetrahydro-3H-3-benzazepine (10a) and 1,2,4,5,6-pentahydro-3H-3-benzazocine (11a) derivatives. Similar treatment of 8 + 9 with water gave 10b and 11b. LAH reduction of 8 + 9 gave 12 and 13b. Compound 10a was converted to 13a and both 13a and 13b were synthesized by a route (14 → 15 → 16 → 13) involving a photocyclization reaction as the key step." @default.
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- W1569093682 date "1971-01-01" @default.
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- W1569093682 title "Reaction of diazomethane with 2-methyl-6,7-methylenedioxy-3,4-dihydro-isoquinolinium perchlorate" @default.
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- W1569093682 doi "https://doi.org/10.1016/s0040-4020(01)91607-2" @default.
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