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- W1569298414 abstract "One of the principal difficulties in investigating mixed-volatile reactions under hydrothermal conditions has been in loading the experimental charges with gas mixtures of known composition. A new technique has been developed based on the fact that solid compounds with pore structures adsorb gases at low temperatures. A gas pipetting apparatus was constructed whereby a known quantity of a gas or gas mixture can be drawn into the experimental capsule by placing it in a low-temperature bath. A solid, such as a zeolite or a gel, is included in the experimental charge. Due to the adsorption of gas by these materials, the resulting vapor pressures are normally <1 mm Hg. The technique is particularly effective for mixtures of non-condensible gases and avoids fractionating the gases between the condensed phase and the coexisting vapors. Synthetic fluid inclusions in quartz, with fluids containing carbon dioxide, methane and water, have been made. Gas chromatography, using a specially designed puncturing device for the capsule, was employed to verify the bulk compositions of the COH gases generated in the experimental charges. Close agreement of the mole ratios of the initial compositions loaded into the experimental capsules and the measured compositions determined after quenching demonstrates the precision of both the gas loading and the gas chromatographic techniques. Mass spectrometry of the contents of individual fluid inclusions yielded results that agreed with these measurements and verified the existence of a homogeneous fluid." @default.
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- W1569298414 date "1989-07-01" @default.
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- W1569298414 title "Hydrothermal reactions involving equilibrium between minerals and mixed volatiles" @default.
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- W1569298414 doi "https://doi.org/10.1016/0009-2541(89)90127-7" @default.
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