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- W1570194310 abstract "Ribonucleosides and their 5′-derivs undergo acid-catalysed exchange with trimethyl orthoacetate and orthobenzoate to give the corresponding 2′,3′-O-methoxy-ethylidene and -benzylidene derivs II (R′ = Me and Ph) respectively. Treatment of the latter with aqueous acids, under very mild conditions, gives mixtures of the respective 2′ (and 3′)-acetates and benzoates, from which it is often possible to obtain a pure crystalline isomer (usually the 3′-ester), in good yield. The orthoester exchange reaction has been applied to the preparation of 3′,5′-di-O-acyl-ribonucleoside derivs, which are required as intermediates in oligoribonucleotide synthesis." @default.
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- W1570194310 date "1967-05-01" @default.
- W1570194310 modified "2023-09-24" @default.
- W1570194310 title "The synthesis of oligoribonucleotides—III" @default.
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- W1570194310 doi "https://doi.org/10.1016/0040-4020(67)80068-1" @default.
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