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- W1570656567 abstract "Abstract A model compound, [ o …-OC 6 H 4 CHNCH 2 C(CH 3 ) 2 NCHC 6 H 4 O…- o ]VO, has been prepared to test the possible effect of steric hindrance. Only 50 percent condensation of the diamine, H 2 NCH 2 C. (CH 3 ) 2 NH 2 , with acetylacetone was indicated, however, and a five-coordinate complex could not be isolated. The model compound shows no discernable tendency toward adduct formation in benzene, pyridine, or dimethylsulfoxide. Attempts to prepare pyridine adducts were unsuccessful though a pyridine derivative of the parent compound VO(salen) was prepared. Attempts to resolve optical enantiomers of the model compound were unsuccessful. Assuming reasonable values for the heat of adduct formation, calorimetric measurements showed that the formation did not occur." @default.
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- W1570656567 date "1970-09-01" @default.
- W1570656567 modified "2023-09-27" @default.
- W1570656567 title "Five-coordinate compounds…-IV" @default.
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- W1570656567 doi "https://doi.org/10.1016/0022-1902(70)80351-7" @default.
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