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- W1570904315 abstract "This chapter focuses on the chemical applications of heteronuclear double resonance. One of the most attractive features of the double-resonance method of measuring the chemical shifts is that a single suitably modified spectrometer can be used for all nuclei, only provided that the 1H or 19F spectrum of the compound studied displays X-1H (X-19F) spin coupling. In many compounds, containing rare isotopic species of low atomic number, especially 13C, the satellite lines of interest in the proton spectrum may be hidden by the strong signal that is provided by the protons in molecules containing non-magnetic isotopes of X. Double-resonance experiments provide an important unequivocal way of comparing the signs. The determination of the absolute sign of a coupling constant cannot be accomplished by double-resonance experiments alone, but there are good reasons for believing that the 13C-1H coupling constant is absolutely positive and a positive value will be adopted in the sequel." @default.
- W1570904315 created "2016-06-24" @default.
- W1570904315 creator A5083759083 @default.
- W1570904315 date "1968-01-01" @default.
- W1570904315 modified "2023-09-25" @default.
- W1570904315 title "Heteronuclear Magnetic Double Resonance" @default.
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- W1570904315 doi "https://doi.org/10.1016/s0066-4103(08)60382-8" @default.
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