Matches in SemOpenAlex for { <https://semopenalex.org/work/W1570908105> ?p ?o ?g. }
Showing items 1 to 77 of
77
with 100 items per page.
- W1570908105 endingPage "577" @default.
- W1570908105 startingPage "572" @default.
- W1570908105 abstract "A method was developed for the determination of 11 anabolic hormones (boldenone, androstenedione, nandrolone, methandrostenolone, methyltestosterone, testosterone, testosterone acetate, trenbolone, testosterone propionate, stanozolol, fluoxymesterone) in fish by multi-function impurity adsorption solid-phase extraction-ultrafast liquid chromatography-tandem mass spectrometry. After the sample was extracted by methanol, the extract was cleaned-up quickly by C18 adsorbent, neutral alumina adsorbent and amino-functionalized nano-adsorbent. The separation was performed on a Shim-Pack XR-ODS II column (100 mm x 2.0 mm, 2.2 microm) using the mobile phases of 0.1% (v/v) formic acid in acetonitrile and 0.1% (v/v) formic acid solution in a gradient elution mode. The identification and quantification were achieved by using electrospray ionization in positive ion mode (ESI+) in multiple reaction monitoring (MRM) mode. The matrix-matched external standard calibration curves were used for quantitative determination. The results showed that the calibration curves were in good linearity for the eleven analytes with the correlation coefficients (r) more than 0.999. The limits of detection (LODs, S/N > 3) for the 11 anabolic hormones were from 0.03 microg/kg to 0.4 microg/kg and the limits of quantification (LOQs, S/N > 10) were from 0.1 microg/kg to 1.5 microg/kg. The average recoveries ranged from 80.9% to 98.1% with the relative standard deviations between 5.2% and 11.5%. The method is simple, rapid, sensitive, accurate and suitable for the quantitative determination and confirmation of the 11 anabolic hormones in fish." @default.
- W1570908105 created "2016-06-24" @default.
- W1570908105 creator A5000069073 @default.
- W1570908105 creator A5005626819 @default.
- W1570908105 creator A5008971453 @default.
- W1570908105 creator A5055974340 @default.
- W1570908105 creator A5065220600 @default.
- W1570908105 date "2013-09-26" @default.
- W1570908105 modified "2023-10-16" @default.
- W1570908105 title "Determination of 11 anabolic hormones in fish tissue by multi- function impurity adsorption solid-phase extraction-ultrafast liquid chromatography-tandem mass spectrometry" @default.
- W1570908105 cites W1966552710 @default.
- W1570908105 cites W1998633907 @default.
- W1570908105 cites W2018024926 @default.
- W1570908105 cites W2021031559 @default.
- W1570908105 cites W2022490922 @default.
- W1570908105 cites W2036219501 @default.
- W1570908105 cites W2041290237 @default.
- W1570908105 cites W2046181413 @default.
- W1570908105 doi "https://doi.org/10.3724/sp.j.1123.2012.02014" @default.
- W1570908105 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23016290" @default.
- W1570908105 hasPublicationYear "2013" @default.
- W1570908105 type Work @default.
- W1570908105 sameAs 1570908105 @default.
- W1570908105 citedByCount "1" @default.
- W1570908105 countsByYear W15709081052022 @default.
- W1570908105 crossrefType "journal-article" @default.
- W1570908105 hasAuthorship W1570908105A5000069073 @default.
- W1570908105 hasAuthorship W1570908105A5005626819 @default.
- W1570908105 hasAuthorship W1570908105A5008971453 @default.
- W1570908105 hasAuthorship W1570908105A5055974340 @default.
- W1570908105 hasAuthorship W1570908105A5065220600 @default.
- W1570908105 hasConcept C119128265 @default.
- W1570908105 hasConcept C162356407 @default.
- W1570908105 hasConcept C185592680 @default.
- W1570908105 hasConcept C23531484 @default.
- W1570908105 hasConcept C2777379063 @default.
- W1570908105 hasConcept C31827203 @default.
- W1570908105 hasConcept C40684141 @default.
- W1570908105 hasConcept C43617362 @default.
- W1570908105 hasConcept C64489805 @default.
- W1570908105 hasConcept C71043704 @default.
- W1570908105 hasConcept C73826308 @default.
- W1570908105 hasConcept C81426234 @default.
- W1570908105 hasConceptScore W1570908105C119128265 @default.
- W1570908105 hasConceptScore W1570908105C162356407 @default.
- W1570908105 hasConceptScore W1570908105C185592680 @default.
- W1570908105 hasConceptScore W1570908105C23531484 @default.
- W1570908105 hasConceptScore W1570908105C2777379063 @default.
- W1570908105 hasConceptScore W1570908105C31827203 @default.
- W1570908105 hasConceptScore W1570908105C40684141 @default.
- W1570908105 hasConceptScore W1570908105C43617362 @default.
- W1570908105 hasConceptScore W1570908105C64489805 @default.
- W1570908105 hasConceptScore W1570908105C71043704 @default.
- W1570908105 hasConceptScore W1570908105C73826308 @default.
- W1570908105 hasConceptScore W1570908105C81426234 @default.
- W1570908105 hasIssue "6" @default.
- W1570908105 hasLocation W15709081051 @default.
- W1570908105 hasLocation W15709081052 @default.
- W1570908105 hasOpenAccess W1570908105 @default.
- W1570908105 hasPrimaryLocation W15709081051 @default.
- W1570908105 hasRelatedWork W1277187992 @default.
- W1570908105 hasRelatedWork W2021034129 @default.
- W1570908105 hasRelatedWork W2082766191 @default.
- W1570908105 hasRelatedWork W2090990910 @default.
- W1570908105 hasRelatedWork W2158733237 @default.
- W1570908105 hasRelatedWork W2352695245 @default.
- W1570908105 hasRelatedWork W2384257091 @default.
- W1570908105 hasRelatedWork W2739744284 @default.
- W1570908105 hasRelatedWork W2972429458 @default.
- W1570908105 hasRelatedWork W3202079152 @default.
- W1570908105 hasVolume "30" @default.
- W1570908105 isParatext "false" @default.
- W1570908105 isRetracted "false" @default.
- W1570908105 magId "1570908105" @default.
- W1570908105 workType "article" @default.