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- W1570950812 abstract "Iron cationic species were generated in the channels of ZSM-5 zeolites by means of exchange procedure performed from aqueous solution with following calcinations at 550 or 900°C. Fe-ZSM-5 samples calcined at 550 and 900° C were characterised by ESR spectroscopy. FT-IR spectra of adsorbed nitric oxide were also recorded. The samples, which demonstrated high activity for benzene hydroxylation (reported in our earlier study) showed ESR signals of iron (III) in the range of low magnetic field (g≈6), which could be easily reduced and subsequently reoxidised by interaction with N2O. Thermal treatment (previous calcinations at 500 or 900°C) influenced significantly the appearance of iron species susceptible to reduction and reoxidation. FT-IR spectra of adsorbed NO showed that calcination temperature of Fe-ZSM-5 affects the formation of different iron complexes, which can be deduced from IR bands of NO adsorbed species." @default.
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- W1570950812 date "2005-01-01" @default.
- W1570950812 modified "2023-10-13" @default.
- W1570950812 title "Iron modified zeolites ZSM-5 studied by ESR spectroscopy" @default.
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- W1570950812 doi "https://doi.org/10.1016/s0167-2991(05)80425-2" @default.
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