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- W1574658895 abstract "The new structure of [Cu2(HCOO)tpmc][Cu2(CH3COO)tpmc](ClO4)6·6H2O (tpmc = N,N′,N″,N‴-tetrakis(2-pyridylmethyl)-1,4,8,11-tetraazacyclotetra-decane), consists of [Cu2(HCOO)tpmc]3+ and [Cu2(CH3COO)tpmc]3+ cations, perchlorate anions and water of crystallization. Two different binuclear transition metal complexes with the tpmc ligand form the same crystal lattice giving the monocrystals. The crystal structure of this compound has been solved by single crystal X-ray diffraction studies. It crystallizes in the triclinic system, space group with a = 14.176(3), Å, b = 16.864(4) Å, c = 20.681(3), Å, α = 100.68(3)○, β = 101.00(3)○, γ = 101.37(3)○, V = 4628.6(16), Å3, R = 0.0729. Each copper atom is penta-coordinated in a distorted square-pyramidal arrangement. In addition, [Cu2(HCOO)tpmc](ClO4)3·H2O was prepared and its properties were compared with the previously described μ-acetato analogue." @default.
- W1574658895 created "2016-06-24" @default.
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- W1574658895 date "2001-08-31" @default.
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- W1574658895 title "SYNTHESIS AND X-RAY CRYSTAL ANALYSIS OF [Cu2(HCOO)tpmc]-[Cu2(CH3COO)tpmc](ClO4)6·6H2O(tpmc = N,N′,N″,N‴-TETRAKIS-(2-PYRIDYLMETHYL)-1,4,8,11-TETRAAZACYCLOTETRADECANE). PREPARATION AND CHARACTERIZATION OF [Cu2(HCOO)tpmc](ClO4)3·H2O" @default.
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- W1574658895 doi "https://doi.org/10.1081/sim-100106857" @default.
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