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- W1574708970 abstract "The tin derivatives of N-acylhydroxylamines, (CH3)2Sn[ON(CH3)COCH3], R2Sn[ON(Ph)COPh]2 (R CH3, PH, n-C4H9, n-C8H17), n-C4H9Sn[ON(Ph)COPh]3, (CH3)3Sn[ON(Ph)SO2C6H4CH3], X2Sn[ON(E)COPh]2 (X Cl, Br, I; E H, Ph), (CH3)2SnX[ON(Ph)COPh] (X Cl, Br, I); Cl2Sn[ON(CH3)COCH3]2 have been prepared. The reaction of N-acetyl-N-methylhydroxylamine with hexamethyldisilazane yielded the trimethylsilyl hydrazine, (CH3)3SiNH—N(CH3)COCH3. From several attempted syntheses of triorganotin derivatives only products of disproportionation were isolated, In particular, (CH3)3Sn[(ON(CH3)COCH3], which could be isolated from the reaction of the hydroxylamine and (CH3)3SnNEt2 in cold ether, disproportionated to (CH3)2Sn[ON(CH3)COCH3]2 and (CH3)4Sn in refluxing ether after 30 min or by heating the solid to ca. 70°C. Tin-119 Mössbauer, vibrational, and mass spectral data are reported for the derivatives and discussed in detail." @default.
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- W1574708970 date "1980-01-01" @default.
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- W1574708970 title "Structural studies in main group chemistry" @default.
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- W1574708970 doi "https://doi.org/10.1016/s0022-328x(00)94399-7" @default.
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