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- W1577067876 abstract "This paper describes the use of cholesteryl-10-undecenoate as a capillary column modifier for capillary electrochromatography. This bonded phase has shown an entirely different selectivity as compared to octadecyl silica (ODS) phases in reversed-phase liquid chromatography, specifically in the analysis of the benzodiazepines. This difference serves as the basis for the continuing study as well as the present focus on electrochromatography as a relatively new separation technique. To significantly increase the surface area, etching of the inner wall of a 75-micron capillary is performed using ammonium hydrogen difluoride and is then subsequently modified via a silation reaction with triethoxysilane and subjected to hydrosilation with cholesteryl-10-undecenoate to form the bonded phase. The performance of this capillary is compared with unetched cholesterol-modified and bare, fused-silica capillaries. Efficient resolution was noted for the etched capillary showing the effectiveness of the etching process as well as the selective property of the bonded phase." @default.
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- W1577067876 date "1999-05-18" @default.
- W1577067876 modified "2023-09-27" @default.
- W1577067876 title "Separation of benzodiazepines using cholesterol-modified fused-silica capillaries in capillary electrochromatography." @default.
- W1577067876 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/10327375" @default.
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