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• W1577559702 abstract "Thermally stimulated current spectroscopy has been applied to the characterization of the structure of amorphous polymers such as polycarbonate. The existence of a sub-T/sub g/ mode that is very sensitive to local order, induced by thermal treatment, has been shown. The dielectric manifestation of the glass transition has been resolved into two components. The lower-temperature one ( alpha /sub 1/) is always observed, independently of the thermodynamic history of the polycarbonate. The corresponding relaxation times follow a compensation law with a compensation temperature given for the reference state by the empirical relationship found for semicrystalline polymers. On the other hand, the upper temperature one ( alpha /sub u/) is only observed after annealing above T/sub g/. It is also characterized by a compensation law indicative of the existence of a segregated phase. It has been assigned to ordered nodules of some 20 to 40 AA, previously observed by electron microscopy and X-ray diffraction. >" @default.
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• W1577559702 date "2003-01-06" @default.
• W1577559702 modified "2023-10-17" @default.
• W1577559702 title "Dielectric spectroscopy of the characterization of the structure of amorphous polymeric materials" @default.
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• W1577559702 doi "https://doi.org/10.1109/icpadm.1988.38504" @default.
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