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- W1583672387 abstract "Abstract Crystals of the bis( tert ‐butyl)silylene (DTBS) derivatives of the tartaric acids were synthesized from D ‐, L ‐, rac ‐, and meso ‐tartaric acid and DTBS bis(trifluoromethanesulfonate): two polymorphs of Si 2 t Bu 4 ( L ‐Tart1,2;3,4H –4 ) ( L ‐ 1a and L ‐ 1b ), the mirror image of the denser modification ( D ‐ 1b ) as well as the racemate ( 2 ), and the meso analogue Si 2 t Bu 4 ( meso ‐Tart1,3;2,4H –4 ) ( 3 ). The structures were determined by single‐crystal X‐ray diffraction. The threo ‐configured D ‐ and L ‐ (and rac ‐) tartrates were coordinated by two t Bu 2 Si units forming five‐membered chelate rings, whereas the erythro ‐configured meso ‐tartrate formed six‐membered chelate rings. The new compounds were analyzed by NMR techniques, including 29 Si NMR spectroscopy, and single‐crystal X‐ray crystallography." @default.
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- W1583672387 date "2013-11-13" @default.
- W1583672387 modified "2023-10-09" @default.
- W1583672387 title "Dibutylsilylene Derivatives of Tartaric Acid" @default.
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- W1583672387 doi "https://doi.org/10.1002/zaac.201300501" @default.
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