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- W1586932877 abstract "Abstract Differential pulse polarography is assessed as amethod for the determination od N -nitrosodiethanolamine (NDEA) in aqueous media. Optimum conditions with respect to pH and supporting electrolyte are found with simple mineral acid solutions (H 2 SO 4 ) at pH 1–2. Detection limits in this medium are of the order 5 × 10 -5 M NDEA. the procedure is applied to the direct determination of NDEA in commercially available grinding fluids which contain, on manufacture, precursors for nitrosamine formation. High concentrations of NDEA were found (75 μM) with an estimated accuracy better than 92% and a precision of ±8%." @default.
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- W1586932877 date "1978-12-01" @default.
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- W1586932877 title "Pulse polarographic determinations of nitrosamines" @default.
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- W1586932877 doi "https://doi.org/10.1016/s0003-2670(01)93467-1" @default.
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