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• W1589910627 abstract "Using 1,2-benzocarbazole-9-ethyl-p-toluenesulfonate (BCETS) as the labeling reagent, a sensitive method for the determination of fatty acids by high performance liquid chromatography (HPLC) with fluorescence detection has been developed. The BCETS could easily and quickly label fatty acids in the presence of the K2CO3 catalyst at 90°C for 30 min in N,N-dimethylformamide solvent. All the tested fatty acid derivatives were separated on a reversed-phase Eclipse XDB-C8 column by HPLC in conjunction with gradient elution. The identification was carried out by post-column atmospheric pressure chemical ionization mass spectrometry (APCI/MS) in positive ion detection mode. The fluorescence excitation and emission wavelengths of the derivatives were at λex 279 nm and λem 380 nm, respectively. Linear correlation coefficients for all fatty acid derivatives are more than 0.9994. Detection limits, at a signal-to-noise ratio of 3:1, were 0.21–0.99 µg/L for the labeled fatty acids. In this study, fatty acids from the ex..." @default.
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• W1589910627 date "2012-08-13" @default.
• W1589910627 modified "2023-09-26" @default.
• W1589910627 title "DETERMINATION AND IDENTIFICATION OF FATTY ACIDS INMICROULA SIKKIMENSISSEED OIL USING 1,2-BENZOCARBAZOLE-9-ETHYL-P-TOLUENESULFONATE AS A NOVEL LABELING REAGENT BY HPLC WITH FLUORESCENCE DETECTION AND APCI-MS" @default.
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• W1589910627 doi "https://doi.org/10.1080/10826076.2011.627621" @default.
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