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• W1592935325 abstract "Convenient and reliable double potential step chronamperometry methods are described for measurement of the rates of protonation of 9-fluorenylidene dianions by carbon acids. The rates of protonation are shown to be insensitive to competing base-catalysed enolisation of the carbon acid. Comparison of experimental i-t transients with those simulated for plausible mechanisms shows that although the measured protonation rate constants are affected by allowing for rapid reproportionation, they are all affected in a similar manner. In contrast, ion-pairing or complexation effects are significant; protonation rate differences caused by varying cation: dianion interactions have been measured and explained. For the dianion of diethyl(4,5-diazafluoren-9-ylidene)malonate a 1:2 complex is formed with Na+ and its formation constant in DMSO has been measured as 1.7 × 108." @default.
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• W1592935325 date "1988-08-01" @default.
• W1592935325 modified "2023-10-17" @default.
• W1592935325 title "Electro-organic reactions" @default.
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• W1592935325 doi "https://doi.org/10.1016/0022-0728(88)85177-5" @default.
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