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- W1593970823 abstract "The influence of the pore diameter and the particle size of silica packing materials on the adsorption of cetyltrimethylammonium (CTMA) ions to its surface when used in high-performance liquid chromatography has been investigated. Adsorption isotherms were determined for ten different silica packing materials having mean pore diameters ranging between 4 and 110 nm and particle sizes of 5 or 10 μm. It was found that the adsorbable amount of CTMA per unit area of the silica surface increases with increasing mean pore diameter of the silica. Silica of narrow pore diameter ranges (4–10 nm) are saturated with CTMA at lower concentrations due to steric hindrance. The particle size of the silica packing material did not exhibit any influence on the amount of CTMA adsorbed per unit area of the silica. The chromatographic retention of fifteen test solutes was determined over the whole range of CTMA concentrations investigated for each of the ten silica packing materials. The retention data proved that the relationship between the solute retention and the amount of CTMA adsorbed onto the silica is dependent on the particle size of the silica packing material. The pore diameter of the silica packing material did not influence the chromatographic selectivity, apart from the effects of a partial exclusion of some test solutes on narrow-pore silica materials due to steric hindrance." @default.
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- W1593970823 date "1986-01-01" @default.
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- W1593970823 title "High-performance liquid chromatography on dynamically modified silica" @default.
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- W1593970823 doi "https://doi.org/10.1016/s0021-9673(00)91651-0" @default.
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