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- W1597377400 abstract "Summary A multiblock copolymer named PDC is composed of crystallizable oligo( p ‐dioxanone) (OPDO) and oligo( ε ‐caprolactone) (OCL) as hard and switching segments. PDC has been synthesized via connecting two oligomeric macrodiols using a diisocyanate linker such as 2,2(4), 4‐trimethyl‐hexamethylene diisocyanate (TMDI) or 1,6‐hexamethylene diisocyanate (HDI). In this work, the surface morphologies of spin coated thin films from two PDCs (PDC‐HDI and PDC‐TMDI) were investigated via in‐situ atomic force microscopy (AFM) to examine how the diisocyanate linkers affect the balance between crystallization and phase segregation behavior. The results demonstrated that in PDC‐HDI, the crystallization of poly( ε ‐caprolactone) (PCL) crystals provoked a “break out” from the phase segregated morphology. On contrary, the crystallization of PCL crystals in PDC‐TMDI was strictly confined in the phase segregated morphology." @default.
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- W1597377400 date "2014-11-01" @default.
- W1597377400 modified "2023-09-23" @default.
- W1597377400 title "Crystallization and Phase Segregation of Multifunctional Multiblock Copolymers in Spin Coated Thin Films Altered by Diurethane Junction Units" @default.
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- W1597377400 doi "https://doi.org/10.1002/masy.201400143" @default.
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