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• W1608842505 abstract "A Ph2P(O)-protected alkyne underwent dephosphorylation by treatment with MeMgBr in THF with Me3Si-protection untouched. The dephosphorylation followed by a transition-metal-catalyzed coupling of the resulting terminal alkyne with aryl halides was carried out in a one-pot manner to afford the desired coupling product. Selective deprotection of Me3Si-/Ph2P(O)-protected alkynes enabled facile syntheses of expanded π-systems such as cyclic phenyleneethynylenes and unsymmetrically substituted ditriazol." @default.
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• W1608842505 date "2014-10-05" @default.
• W1608842505 modified "2023-09-23" @default.
• W1608842505 title "Selective Deprotection of Me₃Si-/Ph₂P(O)-protected Arylalkynes: Methyl Grignard Reagent-promoted Dephosphorylation of Ph₂P(O)-protected Alkynes" @default.
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• W1608842505 doi "https://doi.org/10.1246/cl.140579" @default.
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