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• W1622921104 abstract "Ni1−xO (x<0.001) powders, pure and mixed with pure ZrO2or yttria–partially stabilized zirconia (Y-PSZ), were sintered and then annealed at 1573 and 1873 K for up to 300 h to investigate the dopant dependence of defect clustering in the Ni1−xO lattice. Transmission electron microscopic observations coupled with energy X-ray analysis indicated that the dissolution of Zr4+(ca. 2.0 mol% with or without co-dopant Y3+< 0.3 mol%) but not Ni3+caused defect clustering, which was more rapid at 1873 than 1573 K and which preferred to nucleate at interfaces and dislocations. The paracrystalline distribution of defects was found to be nearly 3.5 and 2.5 times the lattice parameter of Ni1−xO for Zr-doped and (Zr,Y)-codoped Ni1−xO, respectively. The predominantly dissolved Zr4+cations, in octahedral sites with charge- and volume-compensating nickel and oxygen vacancies (i.e., Zroct□nO6−m□m), could create local domains in which Ni3+should be expelled and, thus, in the vicinity the paracrystalline state and then the spinel Ni3O4could precipitate in local domains. The spinelloid, a superstructure of spinel with a relatively high Zr4+content (ca. 3.5 mol%), appeared only for the Ni1−xO particles located at Y-PSZ grain boundaries." @default.
• W1622921104 created "2016-06-24" @default.
• W1622921104 creator A5024981946 @default.
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• W1622921104 date "1998-11-01" @default.
• W1622921104 modified "2023-10-14" @default.
• W1622921104 title "Defect Clusters and Superstructures of Zr4+Dissolved Ni1−xO" @default.
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• W1622921104 doi "https://doi.org/10.1006/jssc.1998.7901" @default.
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