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- W16394089 abstract "Neutron diffraction from single crystals and powders is a powerful technique for investigating the crystal structures of zeolites and microporous materials, as well as other inorganic compounds. Whereas X-ray diffraction is the method by which the framework structures of new zeolites are generally determined, either from a laboratory or synchrotron radiation source, neutrons can be used to probe in greater detail the arrangements of water molecules, hydrogen bonds and cations in the cavities, and the location of adsorbed molecules. The ordering of the tetrahedral atoms of the framework can also be investigated. Neutron diffraction is therefore complementary to other investigative techniques such as magic-angle-spinning NMR. Microporous materials, with the exception of some natural minerals, do not generally form good quality crystals of a size suitable for single-crystal neutron diffraction. Powder diffraction is therefore the technique that is most usually applied. However, for materials where single crystals are available, this is the preferred approach, because the absence of peak overlap greatly enhances the reliability of the refinements of complex structures. The investigation of zeolites by powder neutron diffraction was reviewed in 1986 by Newsam []. This article will review powder work from around this period onwards, as well as previous single-crystal studies. Other articles that are of interest which cover many of the practical aspects of powder diffraction include the reviews by Baerlocher [], Baerlocher and McCusker [], McCusker [, ], and Cheetham and Wilkinson []." @default.
- W16394089 created "2016-06-24" @default.
- W16394089 creator A5027308752 @default.
- W16394089 creator A5078701807 @default.
- W16394089 date "1999-01-01" @default.
- W16394089 modified "2023-10-18" @default.
- W16394089 title "Structural Information from Neutron Diffraction" @default.
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