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- W1640792013 abstract "A series of hydrothermal zeolite synthesis were performed on a powder diffractometer using synchrotron radiation and a position sensitive detector. Direct observation of the induction period(nucleation stage), crystallization and transformation of zeolite 4A(Na-LTA) was possible due to the intense X-ray beam which allows fast data collection. High pressure experiments were performed, allowing observation of hydrothermal synthesis of a cobalt substituted aluminophosphate molecular sieve, CoAPO-5, up to 165°C. The temperature dependence of crystallization rates of CoAPO-5 was studied. At 135°C the crystallization of CoAPO-5 is completed within a few minutes. Rate expressions were fitted to the crystallization curves. A narrowing of the widths of the diffraction peaks was observed during crystallization, signifying crystal growth. A simplified model for the dependence of half width with time was derrived. This is to our knowledge the first time resolved powder diffraction studies of zeolite syntheses using angle dispersive synchrotron powder diffraction." @default.
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- W1640792013 date "1994-01-01" @default.
- W1640792013 modified "2023-09-23" @default.
- W1640792013 title "In situ studies of zeolite syntheses using powder diffraction methods. Crystallization of “instant zeolite A” powder and synthesis of CoAPO-5." @default.
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- W1640792013 doi "https://doi.org/10.1016/s0167-2991(08)64112-9" @default.
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