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- W1645206172 abstract "This paper elaborates the effects of cationic disorder on structural, microstructural and magnetic properties of the Zn0.34Co0.66Fe2O4 nano-particles, synthesised by solvothermal method followed by annealing at 1000°C. The Rietveld refinement of XRD data reveals that nanoparticles are crystallized in spinel structure with Fd-3m space group. The refinement process reveals that the lattice parameter decrease from 8.392 Å to 8.373 Å and Zn2+ ions migrate from octahedral to tetrahedral sites on annealing. Comparison of FESEM microstructures reveals that particle size increase from 30 nm to 200 nm and morphology of the particles changes from spherical to rhombohedral after subjecting them to annealing at 1000°C. The magnetic data analysis shows that magnetization improves significantly from Ms = 47 emu/g to Ms = 64 emu/g at 300 K where as magnetocrystalline anisotropy and coercivity reduces upon annealing. The change in magnetic parameters on annealing is strongly correlated to redistribution of Zn2+ cations on different sites." @default.
- W1645206172 created "2016-06-24" @default.
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- W1645206172 date "2015-01-01" @default.
- W1645206172 modified "2023-10-18" @default.
- W1645206172 title "Effect of Zn2+ migration on microstructural and magnetic properties of nano sized Zn0.34Co0.66Fe2O4 particles" @default.
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- W1645206172 doi "https://doi.org/10.1063/1.4929280" @default.
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