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• W1657368319 startingPage "17" @default.
• W1657368319 abstract "The low-temperature fluorination of a range of insulating alkaline earth cuprates Sr2−xAxCuO3(A=Ca (0≤x≤2);A=Ba (0≤x≤0.6)) can result in superconducting oxide fluorides Sr2−xAxCuO2F2+δ. In contrast, conventional high-temperature solid–state reactions produce thermodynamically more stable mixtures of oxides and fluorides. Various soft-chemistry fluorination pathways (utilizing F2gas, NH4F,MF2[M=Cu, Zn, Ni, Ag]) are compared with respect to their efficacy and mechanisms. Attention is also focused on the structural features of the mixed-oxide precursor and the final-oxide fluorides to highlight the remarkable structural rearrangements that occur during the low-temperature fluorination. The effects of fluorination of other Sr–Cu–O systems are used to identify the structural requirements of the precursor oxide in order to achieve such transformations." @default.
• W1657368319 created "2016-06-24" @default.
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• W1657368319 date "1998-01-01" @default.
• W1657368319 modified "2023-10-17" @default.
• W1657368319 title "Superconducting Sr2−xAxCuO2F2+δ(A=Ca, Ba): Synthetic Pathways and Associated Structural Rearrangements" @default.
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• W1657368319 doi "https://doi.org/10.1006/jssc.1997.7564" @default.
• W1657368319 hasPublicationYear "1998" @default.
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