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- W1662909688 abstract "Electrochemical reduction of in various electrolytes at 150°C has been found to result in the formation of vanadium pentoxide bronzes of formula according to the reaction scheme: with for , respectively. X‐ray diffraction experiments show that bronzes exhibit, at least in the compositional range , an orthorhombic structure closely related to that of the parent oxide. The cationic uptake only induces a slight expansion in the c direction while the a parameter contracts. From chronopotentiometric and voltammetric studies, reversible incorporation of Mn+ ions into is seen to be dependent on the guest cationic species, and is accompanied by a slow diffusion of Na+, K+, and Ca2+ ions in the crystal lattice of the oxide, which prevents utilization of high current densities. These diffusive limitations are mainly responsible for the electrochemical behavior observed and are found to be all the higher as the ionic radius is small, i.e., as the electronic polarizability is low." @default.
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- W1662909688 date "1988-12-01" @default.
- W1662909688 modified "2023-10-14" @default.
- W1662909688 title "Electrochemical Formation of Vanadium Pentoxide Bronzes M x V 2 O 5 in Molten Dimethylsulfone" @default.
- W1662909688 doi "https://doi.org/10.1149/1.2095486" @default.
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