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- W1663722883 abstract "Abstract We grew single crystals of K 1.88 Ga 1.88 Sn 6.12 O 16 hollandite-type compound and precisely determined their crystal structure by X-ray diffraction. K 1.88 Ga 1.88 Sn 6.12 O 16 fibrous crystals measuring an average of about 2 mm in length and 60 μm in diameter were obtained by slow-cooling (from 1623 K to 1273 K) of a flux melt consisting of a 40 mol% crystal composition of (K 2 O) 1 (Ga 2 O 3 ) 1 (SnO 2 ) 1 and a 60 mol% flux composition of (K 2 O) 2 (MoO 3 ) 1 (B 2 O 3 ). The unit cell of K 1.88 Ga 1.88 Sn 6.12 O 16 ( a = 1.0389(2) nm, c = 0.3132(2) nm, V = 0.3381(2) nm 3 ) was larger than that of K 1.52 Ga 1.52 Ti 6.48 O 16 . The ionic size difference with the replacement of Ti by Sn, 10%, was relaxed by an anisotropic expansion of the octahedra by 2.6% in the (001) plane and 5.8% along the c -axis." @default.
- W1663722883 created "2016-06-24" @default.
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- W1663722883 date "2006-10-15" @default.
- W1663722883 modified "2023-10-18" @default.
- W1663722883 title "Crystal growth and refinement of K1.88Ga1.88Sn8.12O16 hollandite-type compound" @default.
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- W1663722883 doi "https://doi.org/10.1016/j.ssi.2006.04.042" @default.
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