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- W1669439391 abstract "(Mo, Nb)13O33 crystallizes in the triclinic system, space group P1 (No. 2). The unit cell dimensions are a = 3.8194(4) Å, b = 11.2898(7) Å, c = 14.9764(9) Å, α = 94.039(5)°, β = 97.326(6)°, γ = 99.748(7)°, V = 628.47(9) Å3, and Z = 1. The structure was refined to R = 0.032, Rw = 0.036, with 1460 observed reflections (I > 3σ(I)) and 186 variable parameters. The structure of (Mo, Nb)13O33 is related to the crystallographic shear structure of the Nb2O5-δ family and is built up from the 3 × 4 × ∞ building blocks of the ReO3-type MO6 octahedra (M = Mo, Nb) and strings of edge-sharing MoO4 tetrahedra running along [101]. The 3 × 4 ReO3-type slabs at different heights along [101] are interconnected through corner sharing with the MoO4 tetrahedra. (Mo, Nb)13O33 is an insulator at room temperature." @default.
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- W1669439391 date "1994-02-01" @default.
- W1669439391 modified "2023-09-25" @default.
- W1669439391 title "Reduced Molybdenum-Niobium Oxides:" @default.
- W1669439391 doi "https://doi.org/10.1006/jssc.1994.1054" @default.
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