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- W16725071 abstract "以1，2-环己二甲酸和异辛醇为原料，浓硫酸为催化剂，酯化合成环保增塑剂环己烷1，2-二甲酸二异辛酯，考察了反应时间、醇酸物质的量比、反应温度等对酯化率的影响，并对产物进行了^1H—NMR、IR、TG及气相定性分析。结果表明，反应时间6h，反应温度170℃，醇酸物质的量比为2．5：1时，酯化率可达99．5％，收率95％，产品为无色油状液体。核磁氢谱显示与酯基相连的亚甲基的多重峰信号8在4．0处，红外谱图显示酯羰基的伸缩振动峰出现在1735cm^-1处，这些结果表明得到了预期产物。产物的TG曲线显示其外延起始温度为215℃，其气相出峰时间为14．310min和14．505min，能够与邻苯二甲酸二异辛酯（DOP）有效分离。" @default.
- W16725071 created "2016-06-24" @default.
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- W16725071 date "2013-01-01" @default.
- W16725071 modified "2023-09-28" @default.
- W16725071 title "环保增塑剂环己烷1，2-二甲酸二异辛酯的合成" @default.
- W16725071 hasPublicationYear "2013" @default.
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