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- W1676940076 abstract "The synthesis of intrazeolite anchoring of [HRuCo3(CO)9(μ2-CO)3] involves the adsorption of metal carbonyl species into zeolite cages followed by reductive carbonylation under a mixed CO and H2 atmosphere. The physicochemical characterization of the samples was based on a multianalytical approach, including Fourier transform-infrared, extended x-ray absorption fine structure spectroscopies, and CO/H2 gas chemisorption. The research encomassed several key points as follows: (a) The generation process of bimetallic carbonyl clusters was considered to occur through the interaction of [Ru–Co], Co(CO)4− and RuI carbonyls, and conversion into [HRuCo3(CO)9(μ3-CO)3] and further to [HRuCo3(CO)9(μ2-CO)3] isomer. (b) There is significant bimetallic interaction. (c) Internal and external confinement of [HRuCo3(CO)9(μ2-CO)3] were compared. (d) The intrazeolite anchoring of [RuCo3] carbonyl clusters shows a strong reaction with the extraframework Na+ α-cage cations, through involvement of the oxygen end of the bridging carbonyl ligands." @default.
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- W1676940076 date "1999-03-22" @default.
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- W1676940076 title "Intrazeolite anchoring of [HRuCo3(CO)9(μ2-CO)3]: Synthesis and reversible decarbonylation" @default.
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- W1676940076 doi "https://doi.org/10.1063/1.478493" @default.
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