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• W1716009308 endingPage "1886" @default.
• W1716009308 startingPage "1880" @default.
• W1716009308 abstract "By reaction of MIICl2·x H2O (M = Fe (x = 4), Co, Ni (x = 6)) and LiOH·H2O in diethylene glycol (DEG) rod-like crystals of the composition MII4Cl4(OCH2CH2OCH2CH2OH)4 are formed. According to X-ray diffraction data obtained by both, single crystals and powders, the CoII and NiII compounds crystallize monoclinic with C2/c (CoII4Cl4(OCH2CH2OCH2CH2OH)4 (1): a = 2084.1(4), b = 919.0(2), c = 1754.0(4) pm, β = 124.3(1)°, Z = 4; NiII4Cl4(OCH2CH2OCH2CH2OH)4 (2): a = 2055.2(4), b = 932.1(2), c = 1727.4(4) pm, β = 125.2(1)°, Z = 4), whereas FeII4Cl4(OCH2CH2OCH2CH2OH)4 (3) crystallizes tetragonal with (a = 1251.4(2), c = 915.3(2) pm, Z = 2). All compounds exhibit analogous molecular structures which are built of a heterocubane-type core consisting of four metal ions and four deprotonated oxygen atoms of four coordinated diethylene glycol molecules. Neutrality of charge is realized by additional coordination of four chloride anions. In addition to the structural characterization, the thermal and magnetical properties of the title compounds are investigated in detail." @default.
• W1716009308 created "2016-06-24" @default.
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• W1716009308 date "2008-09-01" @default.
• W1716009308 modified "2023-10-10" @default.
• W1716009308 title "Drei Heterocubanartige (M^II₄O₄)-Typ Verbindungen (M = Fe^II, Co^II, Ni^II)" @default.
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• W1716009308 doi "https://doi.org/10.1002/zaac.200800203" @default.
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