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- W1717538536 abstract "A series of α- and β-5-halo-2′-deoxyuridine derivatives were prepared with high anomeric selectivity using the conventional silylbase glycosylation method and taking advantage of the 3′-O-(N-acetyl)glycyl protection group and temperature control. Reactions performed at −7 °C gave as much as 87% of the β-anomers, while an overnight reaction at 30 °C gave up to 95% of the α-anomers." @default.
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- W1717538536 date "2015-10-01" @default.
- W1717538536 modified "2023-09-26" @default.
- W1717538536 title "Temperature controlled stereoselectivity in the synthesis of 5-halo-2′-deoxyuridine derivatives" @default.
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- W1717538536 doi "https://doi.org/10.1016/j.tetlet.2015.09.061" @default.
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