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• W1723486069 abstract "Microstructures of 3 mol% yttria‐stabilized zirconia (3YSZ) with different content of TiN were investigated in this study by XRD, SEM, and TEM. The specimens were hot‐pressing sintered at 1450°C for 2.5 h under 50 MPa in vacuum, and then further characterized on microstructure change and phase distribution. The TiN added to 3YSZ can suppress tetragonal ( t ) to monoclinic ( m )‐3YSZ phase transformations, reduce 3YSZ grain size, and improve its mechanical properties. The ceramic was formed of homogeneously dispersed 3YSZ and TiN grains with average size of 0.7 and 1 μm, respectively. The coexistence of t ‐ and m ‐phases was observed in one grain, and the nucleation of m ‐phase with acicular twin occurred preferentially at grain boundaries of t ‐phase. The TEM analysis was focused on the 3YSZ–30 wt% TiN specimens in order to identify the relationships between t ‐ and m ‐structures, and twin structures of m ‐phase. Two crystallographic relations of t ‐ to m ‐transformation are (100) m //(110) t , [010] m //[001] t in type I, and (100) m //(110) t , [001] m //[001] t in the type II. The acicular (100) m and lathlike (110) m twins in m ‐phase were also observed." @default.
• W1723486069 created "2016-06-24" @default.
• W1723486069 creator A5003280063 @default.
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• W1723486069 date "2011-02-28" @default.
• W1723486069 modified "2023-09-26" @default.
• W1723486069 title "The m-t Transformation and Twinning Analysis of Hot-Pressed Sintered 3YSZ Ceramics" @default.
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• W1723486069 doi "https://doi.org/10.1111/j.1551-2916.2010.04347.x" @default.
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