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- W173043024 abstract "Low-temperature rectifying columns without packing were found to be useful for separating small amounts of hydrogen isotopes. The columns are characterized by low entrapment, rapid establishment of equilibrium, and high separating ability at low vapor flow rates. For laboratory urposes the column consisted of a l-mm-diameter glass ube with a 3-cm3 boiler portion at the bottom. A vacuum sleeve surrounded the rectifying portion; the upper section cooled by liquid hydrogen served as the condenser. The unit was placed in a Dewar flask. A 3-component system obtained from the electrolysis of 50% heavy water solution ordinary water served as starting material. It was conensed under vacuum at 1 to 16 deg K. The electric heating as adjusted to provide a vapor flow rate of 1 cm/ sec. The rectification yielded the original mixture of 25% H/sub 2/, 50% HD, and 25% D/sub 2/ with an error of plus or minus 5%. The apparatus is thus useful for analyzing three-component or more complex isotopic mixtures of hydrogen which usually would require the use of a special mass spectrometer. The sharpness of the separation may be improved by reducing the rate. (TTT)" @default.
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- W173043024 date "1962-05-01" @default.
- W173043024 modified "2023-09-24" @default.
- W173043024 title "A MICROCOLUMN FOR SEPARATING AND ANALYZING ISOTOPIC MIXTURES OF HYDROGEN" @default.
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