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• W1750658999 abstract "This paper presents two procedures for the determination of four selective serotonin reuptake inhibitors (citalopram, paroxetine, fluoxetine, and sertraline) and one metabolite (norfluoxetine) in sewage sludge utilizing three-phase hollow fiber liquid-phase microextraction (HF-LPME). First, direct HF-LPME was used for extraction, clean-up, and preconcentration. The pharmaceuticals were extracted from slurry samples into an organic phase and then back-extracted into an aqueous phase in the lumen of the hollow fiber. Second, a procedure combining pressurized hot water extraction and HF-LPME for clean-up and preconcentration was developed for the same analytes and matrix. The extracts were subsequently analyzed by liquid chromatography–mass spectrometry. For direct HF-LPME, limits of detection were between 1 and 12 ng g−1 (dry weight) and the relative standard deviation (RSD) values were 3–12%. For the second method, limits of detection were approximately 6 ng g−1 for all the compounds and RSD values were 8–12%. The methods were validated by comparison of results for the same samples. Sewage sludge from a Swedish wastewater treatment plant was analyzed by both methods; average concentrations were similar for citalopram, paroxetine, and fluoxetine with values of approximately 530, 40, and 200 ng g−1, respectively." @default.
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• W1750658999 date "2012-07-02" @default.
• W1750658999 modified "2023-10-18" @default.
• W1750658999 title "Comparison of two extraction methods for the determination of selective serotonin reuptake inhibitors in sewage sludge by hollow fiber liquid-phase microextraction" @default.
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• W1750658999 doi "https://doi.org/10.1002/jssc.201200257" @default.
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