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• W1752090438 abstract "Two new octadecanuclear clusters [Cu12Ln6(μ3-OH)24(C5H5NCH2CO2)12(H2O)18(μ9-NO3)](PF6)10(NO3)7·12H2O [LnIII=SmIII (1) or GdIII (2)] have been synthesized and characterized by X-ray diffraction. They are isomorphous and crystallize in the triclinic space group P1 with Z=1. The cell dimensions of 1 are a=17.366(1), b=17.790(1), and c=19.002(1) Å, α=117.279(1), β=91.763(1), and γ=111.585(1)°. In the cluster, 6 SmIII atoms are positioned at the vertices of an octahedron, while 12 CuII atoms are at the midpoints of the edges of the octahedron. The CuII–SmIII metal framework is interconnected by the 24 similar μ3-OH− groups, each bridging one SmIII and two CuII atoms. The octahedral cage encapsulates an unusual μ9-NO−3 anion with each oxygen atom coordinated to three CuII atoms. The 12 carboxylate ligands act as μ2-carboxylate-O,O′ bridges, each linking a SmIII and a CuII atom. The PF−6 counteranion plays an important role in crystallization of the two complexes." @default.
• W1752090438 created "2016-06-24" @default.
• W1752090438 creator A5043350702 @default.
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• W1752090438 date "2001-11-01" @default.
• W1752090438 modified "2023-10-16" @default.
• W1752090438 title "Two New Octadecanuclear Copper(II)–Lanthanide(III) Clusters Encapsulating μ9-NO−3 Anions. Synthesis, Structures, and Magnetic Properties of [Cu12Ln6(μ3-OH)24(C5H5NCH2CO2)12(H2O)18(μ9-NO3)](PF6)10(NO3)7·12H2O (LnIII=SmIII or GdIII)" @default.
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• W1752090438 doi "https://doi.org/10.1006/jssc.2001.9300" @default.
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