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- W175952804 abstract "Since the discovery of C60 in 1985 [3], a variety forms of solution grown C60 needle-like crystals with diameters of the order of micrometers ~ ten micrometers have been reported [1, 4, 13, 16]. Contrary to these thick needle-like crystals of C60, various new forms of thin whiskers composed of C60 and C70 fullerene molecules or C60 derivative molecules,“fullerene nanowhiskers”, have been successfully produced by the liquid-liquid interfacial precipitation method (LLIP method) [7−9]. It has been shown that the C60 nanowhiskers are single crystalline, have submicrometer diameters and grow to hundred micrometers ~ millimeter order in length [8, 15]. We have shown that not only the solid nanowhiskers, but also tubular nanowhiskers, “fullerene nanotubes”, composed of fullerene molecules can be prepared by the LLIP method by using pyridine solutions of fullerenes and isopropyl alcohol (IPA) [6, 10, 11]. We can call the fullerene nanowhiskers and fullerene nanotubes “fullerene nanofibers” as well. Thus, the fullerene nanofibers have two kinds of solid and tubular morphologies. In our first paper, X-ray diffraction (XRD) experiments showed that the C60 nanowhiskers prepared by use of the toluene-IPA system and dried at room temperature had a face-centered cubic (fcc) structure [8]. However, we recently found that the as-prepared C60 nanowhiskers had a solvated crystal structure whose lattice constants could be fitted by the hexagonal structure model proposed by Ramm et al. [5, 14]. Further, it was shown that the initially solvated structure of C60 nanowhiskers turned to the fcc structure through the evaporation of contained solvents [5]. It was also Structural characterization of room-temperature synthesized fullerene nanowhiskers Kun’ichi Miyazawa, Jun-ichi Minato, Tadahiko Mashino, Shigeo Nakamura, Masahisa Fujino, Tadatomo Suga" @default.
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- W175952804 date "2006-06-14" @default.
- W175952804 modified "2023-09-30" @default.
- W175952804 title "Structural characterization of room-temperature synthesized fullerene nanowhiskers" @default.
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