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• W1764989721 abstract "Analysis of the chemical composition of surfaces by liquid sampling devices interfaced to mass spectrometry is attractive as the sample stream can be continuously monitored at good sensitivity and selectivity. A sampling probe has been constructed that takes discrete liquid samples (typically <100 nL) of a surface. It incorporates an electrostatic lens system, comprising three electrodes, to which static and pulsed voltages are applied to form a conical “liquid tip”, employed to dissolve analytes at a surface. A prototype system demonstrates spatial resolution of 0.093 mm2. Time of contact between the liquid tip and the surface is controlled to standardize extraction. Calibration graphs of different analyte concentrations on a stainless surface have been measured, together with the probe’s reproducibility, carryover, and recovery. A leucine enkephalin-coated surface demonstrated good linearity (R2 = 0.9936), with a recovery of 90% and a limit of detection of 38 fmol per single spot sampled. The probe is compact and can be fitted into automated sample analysis equipment having potential for rapid analysis of surfaces at a good spatial resolution." @default.
• W1764989721 created "2016-06-24" @default.
• W1764989721 creator A5034933276 @default.
• W1764989721 creator A5083597336 @default.
• W1764989721 date "2014-03-20" @default.
• W1764989721 modified "2023-09-23" @default.
• W1764989721 title "Electro-Focusing Liquid Extractive Surface Analysis (EF-LESA) Coupled to Mass Spectrometry" @default.
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• W1764989721 doi "https://doi.org/10.1021/ac4035136" @default.
• W1764989721 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/3982933" @default.
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• W1764989721 hasPublicationYear "2014" @default.
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