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• W17813356 abstract "The present paper describes and discusses the overcoming of the Cu(II) and Pb(II) interference in the simultaneous voltammetric determination of Os(VIII) and Ru(III) at ultra-trace concentrations. For the determination of all four elements, the method is based on the voltammetric catalytic current of the Os(VIII)-, Ru(III)-, Cu(II)- and Pb(II)-bromate systems and uses a conventional three-electrode cell and 0.5 mol L− 1 acetate buffer pH 4.9 + 5.7 × 10− 2 mol L− 1 NaBrO3 as the supporting electrolyte. The analytical procedure was verified by the analysis of the standard reference materials: Sea Water BCR-CRM 403 and Fresh Water NIST-SRM 1643d. For all the elements, accuracy – expressed as relative error e% – was satisfactory (lower than 6%) while precision as repeatability – expressed as relative standard deviation sr% – was generally lower than 5%. Once set up using the standard reference materials, the analytical procedure was transferred and applied to superficial water samples drawn in proximity to a superhighway and in the area of the mouth of the Po River." @default.
• W17813356 created "2016-06-24" @default.
• W17813356 creator A5042703961 @default.
• W17813356 date "2012-05-01" @default.
• W17813356 modified "2023-09-24" @default.
• W17813356 title "Simultaneous determination of osmium, ruthenium, copper and lead by electrocatalytic voltammetry" @default.
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• W17813356 doi "https://doi.org/10.1016/j.microc.2011.11.009" @default.
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